 
data_FERROFETTELITE
 
_audit_creation_method            JANA2006
_chemical_name_systematic
;
 ?
;
_chemical_name_common             'ferrofettelite'
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'Ag128 As32 Fe4.21 Hg3.79 S120'
_chemical_formula_weight          21047.65
 
loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'Ag'  'Ag'  -0.8971   1.1015
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'S'  'S'   0.1246   0.1234
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'As'  'As'   0.0499   2.0058
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Hg'  'Hg'  -2.3894   9.2266
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Fe'  'Fe'   0.3463   0.8444
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_symmetry_cell_setting            'monoclinic'
_symmetry_space_group_name_H-M    'C2'
 
loop_
 _symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, y, -z'
 'x+1/2, y+1/2, z'
 '-x+1/2, y+1/2, -z'
 
_cell_length_a                    26.011(2)
_cell_length_b                    15.0480(10)
_cell_length_c                    15.5130(10)
_cell_angle_alpha                 90.00
_cell_angle_beta                  90.400(10)
_cell_angle_gamma                 90.00
_cell_volume                      6071.9(7)
_cell_formula_units_Z             1
_cell_measurement_temperature     293(2)
_cell_measurement_reflns_used     2415
_cell_measurement_theta_min       10.5
_cell_measurement_theta_max       27.6
 
_exptl_crystal_description        block
_exptl_crystal_colour             red
_exptl_crystal_size_max           0.078
_exptl_crystal_size_mid           0.072
_exptl_crystal_size_min           0.011
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     5.756
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              9404.8
_exptl_absorpt_coefficient_mu     18.045
_exptl_absorpt_correction_type    'gaussian'
_exptl_absorpt_correction_T_min   0.220
_exptl_absorpt_correction_T_max   0.805
_exptl_absorpt_process_details    
'(ABSPACK; Oxford Diffraction, 2006)'
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       293(2)
_diffrn_radiation_wavelength      0.71069
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source          'fine-focus sealed tube'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type   'Xcalibur 3'
_diffrn_measurement_method        ?
_diffrn_detector_area_resol_mean  ?
_diffrn_standards_number          ?
_diffrn_standards_interval_count  .
_diffrn_standards_interval_time   .
_diffrn_standards_decay_%         ?
_diffrn_reflns_number             70024
_diffrn_reflns_av_R_equivalents   0.0423
_diffrn_reflns_av_sigmaI/netI     0.0398
_diffrn_reflns_limit_h_min        -40
_diffrn_reflns_limit_h_max        41
_diffrn_reflns_limit_k_min        -23
_diffrn_reflns_limit_k_max        23
_diffrn_reflns_limit_l_min        -24
_diffrn_reflns_limit_l_max        24
_diffrn_reflns_theta_min          3.77
_diffrn_reflns_theta_max          34.84
_reflns_number_total              16981
_reflns_number_gt                 8136
_reflns_threshold_expression      >2sigma(I)
 
_computing_data_collection        'CrysAlis (Oxford Diffraction, 2006)'
_computing_cell_refinement        'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction         'CrysAlis (Oxford Diffraction, 2006)'
_computing_structure_solution     'JANA-2006 (Petricek et al., 2006)'
_computing_structure_refinement   'JANA-2006 (Petricek et al., 2006)'
_computing_molecular_graphics     'DIAMOND (Brandenburg, 2001)'
_computing_publication_material   'SHELXL-97 (Sheldrick, 2008)'
 
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
 
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
 'calc w=1/[σ²(Fo²)+(0.0654P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      'known structure'
_atom_sites_solution_secondary    'known structure'
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     .
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        ?
_refine_ls_abs_structure_details
 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack    -0.061(2)
_refine_ls_number_reflns          16981
_refine_ls_number_parameters      659
_refine_ls_number_restraints      1
_refine_ls_R_factor_all           0.0341
_refine_ls_R_factor_gt            0.0314
_refine_ls_wR_factor_ref          0.0696
_refine_ls_wR_factor_gt           0.0682
_refine_ls_goodness_of_fit_ref    0.962
_refine_ls_restrained_S_all       0.962
_refine_ls_shift/su_max           0.003
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Fe1 Fe 0.122901(15) 0.10428(2) 0.501426(18) 0.01752(11) Uani 0.546(2) 1 d P . .
Hg1 Hg 0.122901(15) 0.10428(2) 0.501426(18) 0.01752(11) Uani 0.454(2) 1 d P . .
Fe2 Fe 0.130299(14) 0.61018(2) 0.500109(16) 0.01729(10) Uani 0.506(2) 1 d P . .
Hg2 Hg 0.130299(14) 0.61018(2) 0.500109(16) 0.01729(10) Uani 0.494(2) 1 d P . .
Ag1 Ag 0.28021(2) 0.83512(3) 0.91440(3) 0.02593(10) Uani 1 1 d . . .
Ag2 Ag 0.07835(2) 0.46559(3) 0.08702(3) 0.02467(10) Uani 1 1 d . . .
Ag3 Ag 0.047727(18) 0.61816(3) -0.09586(2) 0.02018(9) Uani 1 1 d . . .
Ag4 Ag -0.028565(18) 0.38326(2) 0.08976(2) 0.01871(8) Uani 1 1 d . . .
Ag5 Ag -0.033039(17) -0.11835(3) 0.08981(2) 0.01957(8) Uani 1 1 d . . .
Ag6 Ag 0.076749(19) -0.02592(3) 0.08682(3) 0.02065(9) Uani 1 1 d . . .
Ag7 Ag 0.046889(17) 0.11624(3) 0.90526(2) 0.01833(8) Uani 1 1 d . . .
Ag8 Ag 0.167034(17) 0.24525(2) 0.91108(2) 0.01903(8) Uani 1 1 d . . .
Ag9 Ag 0.20499(2) 0.09411(3) 0.09844(3) 0.02543(10) Uani 1 1 d . . .
Ag10 Ag 0.281372(19) 0.32277(3) 0.91184(3) 0.02240(9) Uani 1 1 d . . .
Ag11 Ag 0.178361(17) 0.74447(2) 0.91295(2) 0.01897(8) Uani 1 1 d . . .
Ag12 Ag 0.200617(19) 0.60923(3) 0.09394(2) 0.02076(8) Uani 1 1 d . . .
Ag13 Ag 0.12902(2) -0.12902(3) 0.71083(3) 0.02133(8) Uani 1 1 d . . .
Ag14 Ag 0.11669(2) 0.62581(3) 0.30174(3) 0.02276(9) Uani 1 1 d . . .
Ag15 Ag 0.017308(16) 0.72843(2) 0.30764(2) 0.01605(8) Uani 1 1 d . . .
Ag16 Ag 0.014475(17) 0.22697(2) 0.29593(2) 0.01684(7) Uani 1 1 d . . .
Ag17 Ag 0.131611(19) 0.37402(3) 0.70735(2) 0.02002(8) Uani 1 1 d . . .
Ag18 Ag 0.235210(18) 0.48299(3) 0.69742(2) 0.01990(9) Uani 1 1 d . . .
Ag19 Ag 0.11995(2) 0.12830(3) 0.30838(3) 0.02386(9) Uani 1 1 d . . .
Ag20 Ag 0.0000 0.75526(4) 0.5000 0.01891(10) Uani 1 2 d S . .
Ag21 Ag 0.136562(17) 0.07341(2) 0.69020(2) 0.01554(7) Uani 1 1 d . . .
Ag22 Ag 0.183003(16) 0.29319(2) 0.50033(2) 0.01686(8) Uani 1 1 d . . .
Ag23 Ag 0.137532(19) 0.57402(3) 0.69499(2) 0.01912(8) Uani 1 1 d . . .
Ag24 Ag 0.11434(2) 0.32675(3) 0.29817(3) 0.02107(8) Uani 1 1 d . . .
Ag25 Ag 0.178294(18) 0.80086(3) 0.49719(2) 0.02178(9) Uani 1 1 d . . .
Ag26 Ag 0.234617(16) -0.01597(2) 0.69520(2) 0.01659(8) Uani 1 1 d . . .
Ag27 Ag 0.069523(18) -0.08556(3) 0.50162(2) 0.01937(8) Uani 1 1 d . . .
Ag28 Ag 0.116633(19) 0.83269(3) 0.29454(3) 0.02098(9) Uani 1 1 d . . .
Ag29 Ag 0.248024(13) 0.13711(3) 0.501372(13) 0.01682(9) Uani 1 1 d . . .
Ag30 Ag 0.0000 0.28369(4) 0.5000 0.01911(10) Uani 1 2 d S . .
Ag31 Ag 0.248555(12) 0.45515(3) 0.502075(14) 0.01653(9) Uani 1 1 d . . .
Ag32 Ag 0.0000 0.09672(4) 0.5000 0.02402(12) Uani 1 2 d S . .
Ag33 Ag 0.072298(17) 0.41941(3) 0.50040(2) 0.02052(8) Uani 1 1 d . . .
Ag34 Ag 0.0000 0.56031(4) 0.5000 0.01567(9) Uani 1 2 d S . .
As1 As 0.08444(3) 0.22513(4) 0.07232(4) 0.02198(13) Uani 1 1 d . . .
As2 As 0.08084(3) 0.72355(4) 0.07285(3) 0.02030(12) Uani 1 1 d . . .
As3 As 0.16626(3) 0.48536(4) 0.92769(3) 0.01835(12) Uani 1 1 d . . .
As4 As 0.16989(3) -0.01196(4) 0.92668(4) 0.02160(13) Uani 1 1 d . . .
As5 As 0.24901(2) 0.73297(3) 0.28512(3) 0.01703(11) Uani 1 1 d . . .
As6 As 0.00013(2) 0.47190(4) 0.28488(3) 0.01797(12) Uani 1 1 d . . .
As7 As 0.00114(2) -0.02438(3) 0.71439(3) 0.01416(10) Uani 1 1 d . . .
As8 As 0.25028(2) 0.23298(3) 0.28479(3) 0.01498(10) Uani 1 1 d . . .
S1 S 0.00661(6) 0.74554(9) 0.15107(8) 0.0223(2) Uani 1 1 d . . .
S2 S 0.11788(6) 0.11159(10) 0.15381(8) 0.0248(3) Uani 1 1 d . . .
S3 S 0.24226(6) 0.46568(8) 0.85759(7) 0.0178(2) Uani 1 1 d . . .
S4 S 0.13515(5) 0.60325(7) 0.85525(7) 0.0140(2) Uani 1 1 d . . .
S5 S 0.01035(5) 0.24233(7) 0.13887(7) 0.0168(2) Uani 1 1 d . . .
S6 S 0.12487(6) -0.11805(8) 0.87426(8) 0.0202(2) Uani 1 1 d . . .
S7 S 0.12064(6) 0.37808(8) 0.86105(8) 0.0198(3) Uani 1 1 d . . .
S8 S 0.12282(5) 0.83964(7) 0.12975(7) 0.0142(2) Uani 1 1 d . . .
S9 S 0.11306(6) 0.61056(9) 0.14685(7) 0.0191(2) Uani 1 1 d . . .
S10 S 0.12580(6) 0.33539(10) 0.13245(8) 0.0220(3) Uani 1 1 d . . .
S11 S 0.24145(6) -0.02660(8) 0.85481(7) 0.0167(2) Uani 1 1 d . . .
S12 S 0.25443(5) 0.69873(9) -0.00351(5) 0.0190(3) Uani 1 1 d . . .
S13 S 0.13136(5) 0.09774(7) 0.85122(6) 0.0129(2) Uani 1 1 d . . .
S14 S 0.0000 0.51168(9) 0.0000 0.0130(3) Uani 1 2 d S . .
S15 S 0.0000 0.01297(11) 0.0000 0.0200(3) Uani 1 2 d S . .
S16 S 0.21319(6) 0.84667(8) 0.35884(7) 0.0160(2) Uani 1 1 d . . .
S17 S 0.07400(5) -0.02650(7) 0.35289(7) 0.0157(2) Uani 1 1 d . . .
S18 S 0.08550(5) 0.73689(7) 0.46472(6) 0.0156(2) Uani 1 1 d . . .
S19 S 0.08326(5) 0.22844(7) 0.44726(7) 0.0172(2) Uani 1 1 d . . .
S20 S 0.16669(4) -0.02623(6) 0.53039(6) 0.01305(19) Uani 1 1 d . . .
S21 S 0.21299(6) 0.61444(7) 0.35125(7) 0.0147(2) Uani 1 1 d . . .
S22 S 0.07369(5) 0.47227(7) 0.35161(6) 0.01157(19) Uani 1 1 d . . .
S23 S 0.04260(6) -0.13486(8) 0.65087(8) 0.0180(2) Uani 1 1 d . . .
S24 S -0.03842(6) 0.36196(8) 0.34823(7) 0.0147(2) Uani 1 1 d . . .
S25 S -0.03742(6) 0.58788(7) 0.35383(7) 0.0155(2) Uani 1 1 d . . .
S26 S 0.17414(5) 0.23817(7) 0.64448(7) 0.0145(2) Uani 1 1 d . . .
S27 S 0.21099(5) 0.34744(6) 0.35752(6) 0.01060(19) Uani 1 1 d . . .
S28 S 0.28549(6) 0.61957(8) 0.65009(7) 0.0159(2) Uani 1 1 d . . .
S29 S -0.03374(5) 0.08965(6) 0.36107(6) 0.01099(19) Uani 1 1 d . . .
S30 S 0.16878(6) 0.72989(8) 0.64438(7) 0.0178(2) Uani 1 1 d . . .
S31 S 0.16113(4) 0.47849(5) 0.55879(5) 0.01042(16) Uani 1 1 d . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Fe1 S19 2.2908(13) . ?
Fe1 S20 2.3127(10) . ?
Fe1 Ag21 2.9839(5) . ?
Fe1 Ag19 3.0168(5) . ?
Fe1 Ag27 3.1762(5) . ?
Fe2 S18 2.2991(12) . ?
Fe2 S31 2.3213(9) . ?
Fe2 Ag23 3.0763(5) . ?
Fe2 Ag14 3.1040(5) . ?
Fe2 Ag25 3.1297(6) . ?
Ag1 S11 2.4875(14) 1_565 ?
Ag1 S12 2.5091(13) 1_556 ?
Ag1 S10 2.5554(15) 4_556 ?
Ag1 Ag11 2.9797(7) . ?
Ag1 Ag10 3.1506(7) 4_557 ?
Ag1 Ag8 3.3151(7) 4_557 ?
Ag2 S10 2.4180(16) . ?
Ag2 S14 2.5334(7) . ?
Ag2 S9 2.5346(15) . ?
Ag2 Ag4 3.0450(7) . ?
Ag2 Ag4 3.2685(7) 2 ?
Ag3 S4 2.4125(12) 1_554 ?
Ag3 S14 2.5191(9) . ?
Ag3 S1 2.5276(15) 2 ?
Ag4 S5 2.4682(13) . ?
Ag4 S14 2.4979(11) . ?
Ag4 S7 2.5198(14) 2_556 ?
Ag4 Ag4 3.1657(7) 2 ?
Ag4 Ag2 3.2685(7) 2 ?
Ag5 S6 2.4566(15) 2_556 ?
Ag5 S1 2.4796(15) 1_545 ?
Ag5 S15 2.5692(14) . ?
Ag5 Ag6 3.1770(7) . ?
Ag5 Ag6 3.2698(7) 2 ?
Ag5 Ag5 3.2840(7) 2 ?
Ag6 S8 2.4416(13) 1_545 ?
Ag6 S15 2.4707(7) . ?
Ag6 S2 2.5477(17) . ?
Ag6 Ag5 3.2698(7) 2 ?
Ag7 S13 2.3736(12) . ?
Ag7 S15 2.4673(11) 1_556 ?
Ag7 S5 2.5041(13) 2_556 ?
Ag8 S7 2.4579(14) . ?
Ag8 S13 2.5766(12) . ?
Ag8 S12 2.5841(13) 4_546 ?
Ag8 Ag10 3.1945(7) . ?
Ag8 Ag1 3.3151(7) 4_547 ?
Ag9 S12 2.4048(12) 4_545 ?
Ag9 S2 2.4430(15) . ?
Ag9 S3 2.4638(14) 4_546 ?
Ag10 S3 2.5211(14) . ?
Ag10 S12 2.5282(13) 4_546 ?
Ag10 S8 2.5910(13) 4_546 ?
Ag10 Ag11 3.1357(6) 4_547 ?
Ag10 Ag1 3.1506(7) 4_547 ?
Ag10 Ag12 3.2486(7) 4_546 ?
Ag11 S12 2.4562(13) 1_556 ?
Ag11 S6 2.5620(14) 1_565 ?
Ag11 S4 2.5626(13) . ?
Ag11 Ag10 3.1357(6) 4_557 ?
Ag12 S9 2.4262(13) . ?
Ag12 S12 2.4674(12) . ?
Ag12 S11 2.6579(14) 4_556 ?
Ag12 Ag10 3.2486(7) 4_556 ?
Ag13 S23 2.4282(18) . ?
Ag13 S6 2.5438(12) . ?
Ag13 S30 2.5796(11) 1_545 ?
Ag13 Ag21 3.0693(6) . ?
Ag13 Ag26 3.2414(6) . ?
Ag14 S9 2.4150(12) . ?
Ag14 S21 2.6202(17) . ?
Ag14 S22 2.6833(10) . ?
Ag14 Ag15 3.0131(7) . ?
Ag14 Ag28 3.1151(6) . ?
Ag15 S1 2.4562(13) . ?
Ag15 S25 2.6510(12) . ?
Ag15 S23 2.6625(14) 2_566 ?
Ag15 Ag28 3.0306(6) . ?
Ag15 Ag20 3.0479(4) . ?
Ag16 S5 2.4491(12) . ?
Ag16 S24 2.5872(12) . ?
Ag16 S29 2.6232(10) . ?
Ag16 S19 2.9418(15) . ?
Ag16 Ag24 3.0003(7) . ?
Ag16 Ag19 3.1243(7) . ?
Ag16 Ag30 3.3029(4) . ?
Ag17 S7 2.4041(12) . ?
Ag17 S26 2.5237(10) . ?
Ag17 S24 2.5734(17) 2_556 ?
Ag17 S31 2.8978(9) . ?
Ag17 Ag23 3.0196(6) . ?
Ag17 Ag18 3.1591(7) . ?
Ag18 S3 2.5039(12) . ?
Ag18 S28 2.5470(13) . ?
Ag18 S16 2.6053(12) 4_546 ?
Ag18 S31 2.8782(12) . ?
Ag18 Ag23 2.8864(7) . ?
Ag18 Ag31 3.0812(5) . ?
Ag19 S2 2.4112(14) . ?
Ag19 S28 2.5417(17) 4_546 ?
Ag19 S17 2.7097(12) . ?
Ag19 S19 2.8021(11) . ?
Ag19 Ag24 2.9940(6) . ?
Ag20 S18 2.3106(12) . ?
Ag20 S18 2.3106(12) 2_556 ?
Ag20 Ag34 2.9337(7) . ?
Ag20 Ag27 3.0013(7) 1_565 ?
Ag20 Ag27 3.0013(7) 2_566 ?
Ag20 Ag15 3.0479(4) 2_556 ?
Ag21 S13 2.5291(10) . ?
Ag21 S26 2.7596(11) . ?
Ag21 S29 2.7956(15) 2_556 ?
Ag21 Ag26 2.8839(6) . ?
Ag22 S26 2.3971(11) . ?
Ag22 S27 2.4753(9) . ?
Ag22 S19 2.8859(15) . ?
Ag22 Ag29 2.8943(6) . ?
Ag22 Ag31 2.9744(6) . ?
Ag23 S4 2.5259(11) . ?
Ag23 S30 2.6054(12) . ?
Ag23 S31 2.6317(8) . ?
Ag23 S25 2.7148(17) 2_556 ?
Ag24 S22 2.5714(10) . ?
Ag24 S10 2.5934(13) . ?
Ag24 S27 2.6893(15) . ?
Ag24 S19 2.8666(11) . ?
Ag25 S16 2.4356(10) . ?
Ag25 S30 2.5344(12) . ?
Ag25 S18 2.6436(14) . ?
Ag25 S20 2.6700(10) 1_565 ?
Ag25 Ag31 3.0017(7) 4_556 ?
Ag25 Ag29 3.1217(6) 4_556 ?
Ag25 Ag27 3.3065(6) 1_565 ?
Ag26 S11 2.4863(12) . ?
Ag26 S21 2.4983(12) 4_546 ?
Ag26 S27 2.6290(10) 4_546 ?
Ag26 Ag31 3.1248(4) 4_546 ?
Ag27 S17 2.4760(11) . ?
Ag27 S23 2.5345(12) . ?
Ag27 S20 2.7144(12) . ?
Ag27 S18 2.7644(11) 1_545 ?
Ag27 Ag20 3.0013(7) 1_545 ?
Ag27 Ag32 3.2855(7) . ?
Ag27 Ag25 3.3065(6) 1_545 ?
Ag28 S17 2.5599(11) 1_565 ?
Ag28 S8 2.5648(11) . ?
Ag28 S16 2.7041(17) . ?
Ag29 S28 2.5143(14) 4_546 ?
Ag29 S21 2.5178(14) 4_546 ?
Ag29 Ag31 2.7401(7) 4_546 ?
Ag29 Ag25 3.1217(6) 4_546 ?
Ag29 Hg2 3.1910(5) 4_546 ?
Ag30 S19 2.4649(12) . ?
Ag30 S19 2.4649(12) 2_556 ?
Ag30 Ag33 2.7762(6) . ?
Ag30 Ag33 2.7762(6) 2_556 ?
Ag30 S24 2.8101(13) 2_556 ?
Ag30 S24 2.8101(13) . ?
Ag30 Ag32 2.8135(7) . ?
Ag30 Ag16 3.3029(4) 2_556 ?
Ag31 S20 2.2822(11) 4_556 ?
Ag31 S31 2.4690(10) . ?
Ag31 Ag29 2.7401(7) 4_556 ?
Ag31 S16 2.8775(13) 4_546 ?
Ag31 S27 2.9292(11) . ?
Ag31 Ag25 3.0017(7) 4_546 ?
Ag31 Ag26 3.1248(4) 4_556 ?
Ag32 S29 2.3239(12) . ?
Ag32 S29 2.3239(12) 2_556 ?
Ag32 Hg1 3.1987(5) 2_556 ?
Ag32 Ag27 3.2855(7) 2_556 ?
Ag33 S22 2.4419(10) . ?
Ag33 S31 2.6308(12) . ?
Ag33 S24 2.6584(11) 2_556 ?
Ag33 Ag34 2.8340(6) . ?
Ag34 S25 2.4962(13) . ?
Ag34 S25 2.4962(13) 2_556 ?
Ag34 Ag33 2.8340(6) 2_556 ?
As1 S10 2.1832(18) . ?
As1 S5 2.2077(13) . ?
As1 S2 2.2931(18) . ?
As2 S9 2.2130(16) . ?
As2 S8 2.2383(15) . ?
As2 S1 2.3114(13) . ?
As3 S4 2.2476(14) . ?
As3 S7 2.2507(15) . ?
As3 S3 2.2821(13) . ?
As4 S6 2.1374(16) . ?
As4 S11 2.1875(13) . ?
As4 S13 2.2546(14) . ?
As5 S16 2.2624(12) . ?
As5 S21 2.2639(11) . ?
As5 S26 2.2725(16) 4_556 ?
As6 S22 2.1691(14) . ?
As6 S24 2.1730(12) . ?
As6 S25 2.2713(12) . ?
As7 S17 2.2096(16) 2_556 ?
As7 S23 2.2163(13) . ?
As7 S29 2.2466(10) 2_556 ?
As8 S28 2.1935(12) 4_546 ?
As8 S27 2.3021(10) . ?
As8 S30 2.3685(17) 4_546 ?
S1 Ag5 2.4796(15) 1_565 ?
S1 Ag3 2.5276(15) 2 ?
S3 Ag9 2.4638(14) 4_556 ?
S4 Ag3 2.4125(12) 1_556 ?
S5 Ag7 2.5041(13) 2_556 ?
S6 Ag5 2.4566(15) 2_556 ?
S6 Ag11 2.5620(14) 1_545 ?
S7 Ag4 2.5198(14) 2_556 ?
S8 Ag6 2.4416(13) 1_565 ?
S8 Ag10 2.5910(13) 4_556 ?
S10 Ag1 2.5554(15) 4_546 ?
S11 Ag1 2.4875(14) 1_545 ?
S11 Ag12 2.6579(14) 4_546 ?
S12 Ag9 2.4048(12) 4 ?
S12 Ag11 2.4562(13) 1_554 ?
S12 Ag1 2.5091(13) 1_554 ?
S12 Ag10 2.5282(13) 4_556 ?
S12 Ag8 2.5841(13) 4_556 ?
S14 Ag4 2.4979(11) 2 ?
S14 Ag3 2.5191(9) 2 ?
S14 Ag2 2.5334(7) 2 ?
S15 Ag7 2.4673(11) 1_554 ?
S15 Ag7 2.4673(11) 2_556 ?
S15 Ag6 2.4707(7) 2 ?
S15 Ag5 2.5692(14) 2 ?
S16 Ag18 2.6053(12) 4_556 ?
S16 Ag31 2.8775(13) 4_556 ?
S17 As7 2.2096(16) 2_556 ?
S17 Ag28 2.5599(11) 1_545 ?
S18 Ag27 2.7644(11) 1_565 ?
S20 Ag31 2.2822(11) 4_546 ?
S20 Ag25 2.6700(10) 1_545 ?
S21 Ag26 2.4983(12) 4_556 ?
S21 Ag29 2.5178(14) 4_556 ?
S23 Ag15 2.6625(14) 2_546 ?
S24 Ag17 2.5734(17) 2_556 ?
S24 Ag33 2.6584(11) 2_556 ?
S25 Ag23 2.7148(17) 2_556 ?
S26 As5 2.2725(16) 4_546 ?
S27 Ag26 2.6290(10) 4_556 ?
S28 As8 2.1935(12) 4_556 ?
S28 Ag29 2.5143(14) 4_556 ?
S28 Ag19 2.5417(17) 4_556 ?
S29 As7 2.2466(10) 2_556 ?
S29 Ag21 2.7956(15) 2_556 ?
S30 As8 2.3685(17) 4_556 ?
S30 Ag13 2.5796(11) 1_565 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
S19 Fe1 S20 169.61(3) . . ?
S19 Fe1 Ag21 122.49(3) . . ?
S20 Fe1 Ag21 67.79(2) . . ?
S19 Fe1 Ag19 61.96(3) . . ?
S20 Fe1 Ag19 107.68(2) . . ?
Ag21 Fe1 Ag19 174.212(18) . . ?
S19 Fe1 Ag27 122.57(4) . . ?
S20 Fe1 Ag27 56.69(3) . . ?
Ag21 Fe1 Ag27 84.727(13) . . ?
Ag19 Fe1 Ag27 95.774(15) . . ?
S18 Fe2 S31 167.10(3) . . ?
S18 Fe2 Ag23 114.13(3) . . ?
S31 Fe2 Ag23 56.29(2) . . ?
S18 Fe2 Ag14 69.29(3) . . ?
S31 Fe2 Ag14 119.35(2) . . ?
Ag23 Fe2 Ag14 173.441(18) . . ?
S18 Fe2 Ag25 55.79(3) . . ?
S31 Fe2 Ag25 130.66(3) . . ?
Ag23 Fe2 Ag25 98.901(15) . . ?
Ag14 Fe2 Ag25 87.646(14) . . ?
S11 Ag1 S12 139.80(4) 1_565 1_556 ?
S11 Ag1 S10 106.20(5) 1_565 4_556 ?
S12 Ag1 S10 113.91(5) 1_556 4_556 ?
S11 Ag1 Ag11 91.27(4) 1_565 . ?
S12 Ag1 Ag11 52.31(3) 1_556 . ?
S10 Ag1 Ag11 148.31(4) 4_556 . ?
S11 Ag1 Ag10 99.21(3) 1_565 4_557 ?
S12 Ag1 Ag10 51.56(3) 1_556 4_557 ?
S10 Ag1 Ag10 137.44(4) 4_556 4_557 ?
Ag11 Ag1 Ag10 61.454(16) . 4_557 ?
S11 Ag1 Ag8 144.01(3) 1_565 4_557 ?
S12 Ag1 Ag8 50.38(3) 1_556 4_557 ?
S10 Ag1 Ag8 80.88(4) 4_556 4_557 ?
Ag11 Ag1 Ag8 100.506(19) . 4_557 ?
Ag10 Ag1 Ag8 59.153(15) 4_557 4_557 ?
S10 Ag2 S14 141.64(5) . . ?
S10 Ag2 S9 114.26(6) . . ?
S14 Ag2 S9 104.05(5) . . ?
S10 Ag2 Ag4 97.50(4) . . ?
S14 Ag2 Ag4 52.23(3) . . ?
S9 Ag2 Ag4 131.92(4) . . ?
S10 Ag2 Ag4 97.81(4) . 2 ?
S14 Ag2 Ag4 49.02(3) . 2 ?
S9 Ag2 Ag4 140.49(3) . 2 ?
Ag4 Ag2 Ag4 60.064(16) . 2 ?
S4 Ag3 S14 126.58(4) 1_554 . ?
S4 Ag3 S1 119.34(4) 1_554 2 ?
S14 Ag3 S1 113.94(4) . 2 ?
S5 Ag4 S14 135.55(3) . . ?
S5 Ag4 S7 105.58(4) . 2_556 ?
S14 Ag4 S7 118.67(4) . 2_556 ?
S5 Ag4 Ag2 88.93(4) . . ?
S14 Ag4 Ag2 53.289(14) . . ?
S7 Ag4 Ag2 152.48(3) 2_556 . ?
S5 Ag4 Ag4 94.44(2) . 2 ?
S14 Ag4 Ag4 50.68(2) . 2 ?
S7 Ag4 Ag4 136.00(4) 2_556 2 ?
Ag2 Ag4 Ag4 63.472(17) . 2 ?
S5 Ag4 Ag2 138.06(3) . 2 ?
S14 Ag4 Ag2 49.960(13) . 2 ?
S7 Ag4 Ag2 83.91(4) 2_556 2 ?
Ag2 Ag4 Ag2 100.99(2) . 2 ?
Ag4 Ag4 Ag2 56.464(15) 2 2 ?
S6 Ag5 S1 108.48(5) 2_556 1_545 ?
S6 Ag5 S15 116.81(4) 2_556 . ?
S1 Ag5 S15 134.70(4) 1_545 . ?
S6 Ag5 Ag6 151.41(3) 2_556 . ?
S1 Ag5 Ag6 89.76(4) 1_545 . ?
S15 Ag5 Ag6 49.555(12) . . ?
S6 Ag5 Ag6 81.74(4) 2_556 2 ?
S1 Ag5 Ag6 144.47(3) 1_545 2 ?
S15 Ag5 Ag6 48.248(12) . 2 ?
Ag6 Ag5 Ag6 96.250(19) . 2 ?
S6 Ag5 Ag5 135.07(4) 2_556 2 ?
S1 Ag5 Ag5 96.11(3) 1_545 2 ?
S15 Ag5 Ag5 50.27(3) . 2 ?
Ag6 Ag5 Ag5 60.778(15) . 2 ?
Ag6 Ag5 Ag5 57.993(14) 2 2 ?
S8 Ag6 S15 137.57(5) 1_545 . ?
S8 Ag6 S2 110.97(5) 1_545 . ?
S15 Ag6 S2 111.43(6) . . ?
S8 Ag6 Ag5 94.17(3) 1_545 . ?
S15 Ag6 Ag5 52.32(3) . . ?
S2 Ag6 Ag5 136.43(4) . . ?
S8 Ag6 Ag5 92.48(3) 1_545 2 ?
S15 Ag6 Ag5 50.88(3) . 2 ?
S2 Ag6 Ag5 146.09(3) . 2 ?
Ag5 Ag6 Ag5 61.229(16) . 2 ?
S13 Ag7 S15 126.81(4) . 1_556 ?
S13 Ag7 S5 122.85(4) . 2_556 ?
S15 Ag7 S5 110.16(4) 1_556 2_556 ?
S7 Ag8 S13 114.33(5) . . ?
S7 Ag8 S12 141.26(5) . 4_546 ?
S13 Ag8 S12 104.35(4) . 4_546 ?
S7 Ag8 Ag10 99.16(3) . . ?
S13 Ag8 Ag10 130.45(3) . . ?
S12 Ag8 Ag10 50.55(3) 4_546 . ?
S7 Ag8 Ag1 97.22(4) . 4_547 ?
S13 Ag8 Ag1 142.35(3) . 4_547 ?
S12 Ag8 Ag1 48.41(3) 4_546 4_547 ?
Ag10 Ag8 Ag1 57.858(15) . 4_547 ?
S12 Ag9 S2 123.84(5) 4_545 . ?
S12 Ag9 S3 115.92(5) 4_545 4_546 ?
S2 Ag9 S3 120.21(5) . 4_546 ?
S3 Ag10 S12 131.92(4) . 4_546 ?
S3 Ag10 S8 102.70(4) . 4_546 ?
S12 Ag10 S8 124.83(5) 4_546 4_546 ?
S3 Ag10 Ag11 137.85(3) . 4_547 ?
S12 Ag10 Ag11 50.00(3) 4_546 4_547 ?
S8 Ag10 Ag11 86.37(3) 4_546 4_547 ?
S3 Ag10 Ag1 91.65(3) . 4_547 ?
S12 Ag10 Ag1 51.01(3) 4_546 4_547 ?
S8 Ag10 Ag1 134.66(4) 4_546 4_547 ?
Ag11 Ag10 Ag1 56.587(15) 4_547 4_547 ?
S3 Ag10 Ag8 86.37(4) . . ?
S12 Ag10 Ag8 52.11(3) 4_546 . ?
S8 Ag10 Ag8 158.73(3) 4_546 . ?
Ag11 Ag10 Ag8 99.865(17) 4_547 . ?
Ag1 Ag10 Ag8 62.989(16) 4_547 . ?
S3 Ag10 Ag12 153.18(4) . 4_546 ?
S12 Ag10 Ag12 48.63(3) 4_546 4_546 ?
S8 Ag10 Ag12 87.19(3) 4_546 4_546 ?
Ag11 Ag10 Ag12 66.729(14) 4_547 4_546 ?
Ag1 Ag10 Ag12 98.990(13) 4_547 4_546 ?
Ag8 Ag10 Ag12 76.889(15) . 4_546 ?
S12 Ag11 S6 141.63(5) 1_556 1_565 ?
S12 Ag11 S4 107.56(5) 1_556 . ?
S6 Ag11 S4 110.59(5) 1_565 . ?
S12 Ag11 Ag1 53.94(3) 1_556 . ?
S6 Ag11 Ag1 96.52(4) 1_565 . ?
S4 Ag11 Ag1 140.36(3) . . ?
S12 Ag11 Ag10 52.05(3) 1_556 4_557 ?
S6 Ag11 Ag10 94.43(3) 1_565 4_557 ?
S4 Ag11 Ag10 139.24(3) . 4_557 ?
Ag1 Ag11 Ag10 61.959(16) . 4_557 ?
S9 Ag12 S12 137.79(5) . . ?
S9 Ag12 S11 115.89(4) . 4_556 ?
S12 Ag12 S11 106.27(4) . 4_556 ?
S9 Ag12 Ag10 97.88(4) . 4_556 ?
S12 Ag12 Ag10 50.26(3) . 4_556 ?
S11 Ag12 Ag10 133.42(4) 4_556 4_556 ?
S23 Ag13 S6 109.79(5) . . ?
S23 Ag13 S30 100.94(5) . 1_545 ?
S6 Ag13 S30 118.14(5) . 1_545 ?
S23 Ag13 Ag21 93.19(4) . . ?
S6 Ag13 Ag21 92.45(3) . . ?
S30 Ag13 Ag21 138.51(3) 1_545 . ?
S23 Ag13 Ag26 140.62(3) . . ?
S6 Ag13 Ag26 94.72(4) . . ?
S30 Ag13 Ag26 93.42(3) 1_545 . ?
Ag21 Ag13 Ag26 54.302(13) . . ?
S9 Ag14 S21 108.43(4) . . ?
S9 Ag14 S22 101.04(4) . . ?
S21 Ag14 S22 105.00(4) . . ?
S9 Ag14 Ag15 92.94(4) . . ?
S21 Ag14 Ag15 147.47(3) . . ?
S22 Ag14 Ag15 94.19(3) . . ?
S9 Ag14 Fe2 169.30(4) . . ?
S21 Ag14 Fe2 66.57(3) . . ?
S22 Ag14 Fe2 72.17(3) . . ?
Ag15 Ag14 Fe2 95.778(16) . . ?
S9 Ag14 Ag28 93.40(4) . . ?
S21 Ag14 Ag28 94.36(3) . . ?
S22 Ag14 Ag28 150.55(3) . . ?
Ag15 Ag14 Ag28 59.250(15) . . ?
Fe2 Ag14 Ag28 96.391(17) . . ?
S1 Ag15 S25 107.07(5) . . ?
S1 Ag15 S23 95.49(4) . 2_566 ?
S25 Ag15 S23 103.58(4) . 2_566 ?
S1 Ag15 Ag14 96.61(4) . . ?
S25 Ag15 Ag14 93.54(3) . . ?
S23 Ag15 Ag14 155.10(4) 2_566 . ?
S1 Ag15 Ag28 88.29(4) . . ?
S25 Ag15 Ag28 152.97(4) . . ?
S23 Ag15 Ag28 96.71(3) 2_566 . ?
Ag14 Ag15 Ag28 62.051(15) . . ?
S1 Ag15 Ag20 159.68(4) . . ?
S25 Ag15 Ag20 75.98(3) . . ?
S23 Ag15 Ag20 64.55(3) 2_566 . ?
Ag14 Ag15 Ag20 103.310(18) . . ?
Ag28 Ag15 Ag20 97.404(17) . . ?
S5 Ag16 S24 102.60(4) . . ?
S5 Ag16 S29 116.09(4) . . ?
S24 Ag16 S29 103.94(3) . . ?
S5 Ag16 S19 144.63(4) . . ?
S24 Ag16 S19 93.77(4) . . ?
S29 Ag16 S19 89.33(4) . . ?
S5 Ag16 Ag24 89.78(3) . . ?
S24 Ag16 Ag24 93.77(3) . . ?
S29 Ag16 Ag24 143.70(4) . . ?
S19 Ag16 Ag24 57.68(2) . . ?
S5 Ag16 Ag19 97.97(3) . . ?
S24 Ag16 Ag19 145.33(4) . . ?
S29 Ag16 Ag19 91.36(3) . . ?
S19 Ag16 Ag19 54.92(2) . . ?
Ag24 Ag16 Ag19 58.488(15) . . ?
S5 Ag16 Ag30 157.62(3) . . ?
S24 Ag16 Ag30 55.40(3) . . ?
S29 Ag16 Ag30 77.08(2) . . ?
S19 Ag16 Ag30 46.05(2) . . ?
Ag24 Ag16 Ag30 87.938(16) . . ?
Ag19 Ag16 Ag30 99.757(17) . . ?
S7 Ag17 S26 117.34(5) . . ?
S7 Ag17 S24 102.47(5) . 2_556 ?
S26 Ag17 S24 103.17(4) . 2_556 ?
S7 Ag17 S31 143.99(4) . . ?
S26 Ag17 S31 90.73(3) . . ?
S24 Ag17 S31 91.49(4) 2_556 . ?
S7 Ag17 Ag23 92.53(3) . . ?
S26 Ag17 Ag23 139.47(3) . . ?
S24 Ag17 Ag23 95.59(3) 2_556 . ?
S31 Ag17 Ag23 52.764(18) . . ?
S7 Ag17 Ag18 98.19(4) . . ?
S26 Ag17 Ag18 91.45(3) . . ?
S24 Ag17 Ag18 145.29(3) 2_556 . ?
S31 Ag17 Ag18 56.55(2) . . ?
Ag23 Ag17 Ag18 55.645(14) . . ?
S3 Ag18 S28 109.63(5) . . ?
S3 Ag18 S16 102.49(4) . 4_546 ?
S28 Ag18 S16 105.79(4) . 4_546 ?
S3 Ag18 S31 141.54(4) . . ?
S28 Ag18 S31 98.39(4) . . ?
S16 Ag18 S31 94.30(4) 4_546 . ?
S3 Ag18 Ag23 96.93(3) . . ?
S28 Ag18 Ag23 93.84(3) . . ?
S16 Ag18 Ag23 145.56(4) 4_546 . ?
S31 Ag18 Ag23 54.32(2) . . ?
S3 Ag18 Ag31 162.53(3) . . ?
S28 Ag18 Ag31 76.39(3) . . ?
S16 Ag18 Ag31 60.11(3) 4_546 . ?
S31 Ag18 Ag31 48.805(19) . . ?
Ag23 Ag18 Ag31 99.027(19) . . ?
S3 Ag18 Ag17 87.37(3) . . ?
S28 Ag18 Ag17 150.79(4) . . ?
S16 Ag18 Ag17 92.82(3) 4_546 . ?
S31 Ag18 Ag17 57.14(2) . . ?
Ag23 Ag18 Ag17 59.728(15) . . ?
Ag31 Ag18 Ag17 94.553(18) . . ?
S2 Ag19 S28 105.16(5) . 4_546 ?
S2 Ag19 S17 99.03(5) . . ?
S28 Ag19 S17 108.59(4) 4_546 . ?
S2 Ag19 S19 144.62(5) . . ?
S28 Ag19 S19 99.62(4) 4_546 . ?
S17 Ag19 S19 96.50(3) . . ?
S2 Ag19 Ag24 92.90(4) . . ?
S28 Ag19 Ag24 96.41(3) 4_546 . ?
S17 Ag19 Ag24 148.16(3) . . ?
S19 Ag19 Ag24 59.17(3) . . ?
S2 Ag19 Fe1 167.13(4) . . ?
S28 Ag19 Fe1 74.00(3) 4_546 . ?
S17 Ag19 Fe1 69.65(3) . . ?
S19 Ag19 Fe1 46.18(3) . . ?
Ag24 Ag19 Fe1 99.957(17) . . ?
S2 Ag19 Ag16 88.54(4) . . ?
S28 Ag19 Ag16 152.63(3) 4_546 . ?
S17 Ag19 Ag16 92.04(3) . . ?
S19 Ag19 Ag16 59.23(3) . . ?
Ag24 Ag19 Ag16 58.686(16) . . ?
Fe1 Ag19 Ag16 97.734(17) . . ?
S18 Ag20 S18 166.26(6) . 2_556 ?
S18 Ag20 Ag34 83.13(3) . . ?
S18 Ag20 Ag34 83.13(3) 2_556 . ?
S18 Ag20 Ag27 61.09(3) . 1_565 ?
S18 Ag20 Ag27 132.41(3) 2_556 1_565 ?
Ag34 Ag20 Ag27 142.949(12) . 1_565 ?
S18 Ag20 Ag27 132.41(3) . 2_566 ?
S18 Ag20 Ag27 61.09(3) 2_556 2_566 ?
Ag34 Ag20 Ag27 142.949(12) . 2_566 ?
Ag27 Ag20 Ag27 74.10(2) 1_565 2_566 ?
S18 Ag20 Ag15 66.63(3) . . ?
S18 Ag20 Ag15 111.41(3) 2_556 . ?
Ag34 Ag20 Ag15 82.387(14) . . ?
Ag27 Ag20 Ag15 91.193(14) 1_565 . ?
Ag27 Ag20 Ag15 100.990(15) 2_566 . ?
S18 Ag20 Ag15 111.41(3) . 2_556 ?
S18 Ag20 Ag15 66.63(3) 2_556 2_556 ?
Ag34 Ag20 Ag15 82.387(14) . 2_556 ?
Ag27 Ag20 Ag15 100.990(15) 1_565 2_556 ?
Ag27 Ag20 Ag15 91.193(14) 2_566 2_556 ?
Ag15 Ag20 Ag15 164.77(3) . 2_556 ?
S13 Ag21 S26 98.35(3) . . ?
S13 Ag21 S29 102.16(4) . 2_556 ?
S26 Ag21 S29 100.85(4) . 2_556 ?
S13 Ag21 Ag26 95.42(3) . . ?
S26 Ag21 Ag26 96.38(3) . . ?
S29 Ag21 Ag26 153.20(3) 2_556 . ?
S13 Ag21 Fe1 160.04(3) . . ?
S26 Ag21 Fe1 69.38(3) . . ?
S29 Ag21 Fe1 66.42(2) 2_556 . ?
Ag26 Ag21 Fe1 101.433(15) . . ?
S13 Ag21 Ag13 92.11(3) . . ?
S26 Ag21 Ag13 160.30(3) . . ?
S29 Ag21 Ag13 93.14(2) 2_556 . ?
Ag26 Ag21 Ag13 65.893(15) . . ?
Fe1 Ag21 Ag13 104.452(15) . . ?
S26 Ag22 S27 168.42(5) . . ?
S26 Ag22 S19 93.29(4) . . ?
S27 Ag22 S19 97.20(4) . . ?
S26 Ag22 Ag29 76.97(3) . . ?
S27 Ag22 Ag29 95.57(3) . . ?
S19 Ag22 Ag29 104.58(3) . . ?
S26 Ag22 Ag31 109.48(3) . . ?
S27 Ag22 Ag31 64.26(3) . . ?
S19 Ag22 Ag31 142.50(3) . . ?
Ag29 Ag22 Ag31 109.267(18) . . ?
S4 Ag23 S30 98.61(4) . . ?
S4 Ag23 S31 153.23(4) . . ?
S30 Ag23 S31 100.07(3) . . ?
S4 Ag23 S25 103.36(4) . 2_556 ?
S30 Ag23 S25 98.48(4) . 2_556 ?
S31 Ag23 S25 92.68(4) . 2_556 ?
S4 Ag23 Ag18 95.59(4) . . ?
S30 Ag23 Ag18 98.90(3) . . ?
S31 Ag23 Ag18 62.68(3) . . ?
S25 Ag23 Ag18 151.96(3) 2_556 . ?
S4 Ag23 Ag17 96.29(3) . . ?
S30 Ag23 Ag17 158.84(3) . . ?
S31 Ag23 Ag17 61.24(2) . . ?
S25 Ag23 Ag17 92.58(3) 2_556 . ?
Ag18 Ag23 Ag17 64.627(16) . . ?
S4 Ag23 Fe2 159.18(3) . . ?
S30 Ag23 Fe2 64.00(3) . . ?
S31 Ag23 Fe2 47.20(2) . . ?
S25 Ag23 Fe2 70.14(3) 2_556 . ?
Ag18 Ag23 Fe2 98.311(16) . . ?
Ag17 Ag23 Fe2 103.645(16) . . ?
S22 Ag24 S10 109.10(4) . . ?
S22 Ag24 S27 100.17(4) . . ?
S10 Ag24 S27 102.70(4) . . ?
S22 Ag24 S19 93.47(3) . . ?
S10 Ag24 S19 149.39(4) . . ?
S27 Ag24 S19 92.97(4) . . ?
S22 Ag24 Ag19 148.46(3) . . ?
S10 Ag24 Ag19 95.54(3) . . ?
S27 Ag24 Ag19 92.99(3) . . ?
S19 Ag24 Ag19 57.08(2) . . ?
S22 Ag24 Ag16 94.13(3) . . ?
S10 Ag24 Ag16 96.84(4) . . ?
S27 Ag24 Ag16 150.35(3) . . ?
S19 Ag24 Ag16 60.14(3) . . ?
Ag19 Ag24 Ag16 62.826(17) . . ?
S16 Ag25 S30 162.26(5) . . ?
S16 Ag25 S18 106.29(5) . . ?
S30 Ag25 S18 85.61(4) . . ?
S16 Ag25 S20 86.42(3) . 1_565 ?
S30 Ag25 S20 103.00(3) . 1_565 ?
S18 Ag25 S20 106.70(3) . 1_565 ?
S16 Ag25 Ag31 62.89(3) . 4_556 ?
S30 Ag25 Ag31 112.85(4) . 4_556 ?
S18 Ag25 Ag31 149.34(3) . 4_556 ?
S20 Ag25 Ag31 47.00(3) 1_565 4_556 ?
S16 Ag25 Ag29 89.84(3) . 4_556 ?
S30 Ag25 Ag29 74.02(3) . 4_556 ?
S18 Ag25 Ag29 105.88(3) . 4_556 ?
S20 Ag25 Ag29 146.94(3) 1_565 4_556 ?
Ag31 Ag25 Ag29 102.791(18) 4_556 4_556 ?
S16 Ag25 Fe2 115.05(3) . . ?
S30 Ag25 Fe2 63.84(3) . . ?
S18 Ag25 Fe2 45.99(3) . . ?
S20 Ag25 Fe2 147.68(3) 1_565 . ?
Ag31 Ag25 Fe2 164.15(2) 4_556 . ?
Ag29 Ag25 Fe2 61.387(13) 4_556 . ?
S16 Ag25 Ag27 101.31(4) . 1_565 ?
S30 Ag25 Ag27 96.33(3) . 1_565 ?
S18 Ag25 Ag27 53.98(3) . 1_565 ?
S20 Ag25 Ag27 52.72(3) 1_565 1_565 ?
Ag31 Ag25 Ag27 98.197(16) 4_556 1_565 ?
Ag29 Ag25 Ag27 158.944(18) 4_556 1_565 ?
Fe2 Ag25 Ag27 97.594(16) . 1_565 ?
S11 Ag26 S21 107.60(4) . 4_546 ?
S11 Ag26 S27 102.98(4) . 4_546 ?
S21 Ag26 S27 103.21(3) 4_546 4_546 ?
S11 Ag26 Ag21 96.54(3) . . ?
S21 Ag26 Ag21 96.32(4) 4_546 . ?
S27 Ag26 Ag21 146.51(3) 4_546 . ?
S11 Ag26 Ag31 163.10(3) . 4_546 ?
S21 Ag26 Ag31 75.31(3) 4_546 4_546 ?
S27 Ag26 Ag31 60.48(2) 4_546 4_546 ?
Ag21 Ag26 Ag31 99.698(17) . 4_546 ?
S11 Ag26 Ag13 86.93(3) . . ?
S21 Ag26 Ag13 153.91(4) 4_546 . ?
S27 Ag26 Ag13 94.07(3) 4_546 . ?
Ag21 Ag26 Ag13 59.805(14) . . ?
Ag31 Ag26 Ag13 97.170(17) 4_546 . ?
S17 Ag27 S23 166.26(5) . . ?
S17 Ag27 S20 89.16(4) . . ?
S23 Ag27 S20 102.06(5) . . ?
S17 Ag27 S18 98.39(3) . 1_545 ?
S23 Ag27 S18 87.08(4) . 1_545 ?
S20 Ag27 S18 102.17(4) . 1_545 ?
S17 Ag27 Ag20 108.11(3) . 1_545 ?
S23 Ag27 Ag20 66.66(4) . 1_545 ?
S20 Ag27 Ag20 145.50(3) . 1_545 ?
S18 Ag27 Ag20 47.03(3) 1_545 1_545 ?
S17 Ag27 Fe1 69.69(3) . . ?
S23 Ag27 Fe1 112.81(3) . . ?
S20 Ag27 Fe1 45.40(2) . . ?
S18 Ag27 Fe1 143.39(3) 1_545 . ?
Ag20 Ag27 Fe1 168.86(2) 1_545 . ?
S17 Ag27 Ag32 73.90(3) . . ?
S23 Ag27 Ag32 95.50(3) . . ?
S20 Ag27 Ag32 103.79(2) . . ?
S18 Ag27 Ag32 152.73(3) 1_545 . ?
Ag20 Ag27 Ag32 109.553(17) 1_545 . ?
Fe1 Ag27 Ag32 59.315(12) . . ?
S17 Ag27 Ag25 96.91(3) . 1_545 ?
S23 Ag27 Ag25 96.29(4) . 1_545 ?
S20 Ag27 Ag25 51.51(2) . 1_545 ?
S18 Ag27 Ag25 50.67(3) 1_545 1_545 ?
Ag20 Ag27 Ag25 95.905(16) 1_545 1_545 ?
Fe1 Ag27 Ag25 95.208(16) . 1_545 ?
Ag32 Ag27 Ag25 154.474(16) . 1_545 ?
S17 Ag28 S8 110.43(4) 1_565 . ?
S17 Ag28 S16 102.04(5) 1_565 . ?
S8 Ag28 S16 107.45(4) . . ?
S17 Ag28 Ag15 91.90(3) 1_565 . ?
S8 Ag28 Ag15 98.48(4) . . ?
S16 Ag28 Ag15 143.67(3) . . ?
S17 Ag28 Ag14 144.55(3) 1_565 . ?
S8 Ag28 Ag14 94.39(3) . . ?
S16 Ag28 Ag14 93.69(3) . . ?
Ag15 Ag28 Ag14 58.700(16) . . ?
S28 Ag29 S21 165.73(5) 4_546 4_546 ?
S28 Ag29 Ag31 83.57(3) 4_546 4_546 ?
S21 Ag29 Ag31 82.50(3) 4_546 4_546 ?
S28 Ag29 Ag22 83.18(3) 4_546 . ?
S21 Ag29 Ag22 110.28(3) 4_546 . ?
Ag31 Ag29 Ag22 146.086(17) 4_546 . ?
S28 Ag29 Ag25 107.36(3) 4_546 4_546 ?
S21 Ag29 Ag25 81.78(3) 4_546 4_546 ?
Ag31 Ag29 Ag25 140.256(17) 4_546 4_546 ?
Ag22 Ag29 Ag25 73.630(19) . 4_546 ?
S28 Ag29 Hg2 108.50(3) 4_546 4_546 ?
S21 Ag29 Hg2 66.18(3) 4_546 4_546 ?
Ag31 Ag29 Hg2 80.829(13) 4_546 4_546 ?
Ag22 Ag29 Hg2 133.045(18) . 4_546 ?
Ag25 Ag29 Hg2 59.428(12) 4_546 4_546 ?
S19 Ag30 S19 140.57(6) . 2_556 ?
S19 Ag30 Ag33 69.65(3) . . ?
S19 Ag30 Ag33 147.58(3) 2_556 . ?
S19 Ag30 Ag33 147.58(3) . 2_556 ?
S19 Ag30 Ag33 69.65(3) 2_556 2_556 ?
Ag33 Ag30 Ag33 85.28(3) . 2_556 ?
S19 Ag30 S24 96.39(4) . 2_556 ?
S19 Ag30 S24 99.87(4) 2_556 2_556 ?
Ag33 Ag30 S24 56.83(2) . 2_556 ?
Ag33 Ag30 S24 86.01(3) 2_556 2_556 ?
S19 Ag30 S24 99.87(4) . . ?
S19 Ag30 S24 96.39(4) 2_556 . ?
Ag33 Ag30 S24 86.01(3) . . ?
Ag33 Ag30 S24 56.83(2) 2_556 . ?
S24 Ag30 S24 130.44(5) 2_556 . ?
S19 Ag30 Ag32 70.29(3) . . ?
S19 Ag30 Ag32 70.29(3) 2_556 . ?
Ag33 Ag30 Ag32 137.362(13) . . ?
Ag33 Ag30 Ag32 137.362(13) 2_556 . ?
S24 Ag30 Ag32 114.78(3) 2_556 . ?
S24 Ag30 Ag32 114.78(3) . . ?
S19 Ag30 Ag16 59.23(3) . . ?
S19 Ag30 Ag16 109.71(3) 2_556 . ?
Ag33 Ag30 Ag16 96.344(13) . . ?
Ag33 Ag30 Ag16 105.648(14) 2_556 . ?
S24 Ag30 Ag16 150.36(3) 2_556 . ?
S24 Ag30 Ag16 49.27(2) . . ?
Ag32 Ag30 Ag16 75.023(12) . . ?
S19 Ag30 Ag16 109.71(3) . 2_556 ?
S19 Ag30 Ag16 59.23(3) 2_556 2_556 ?
Ag33 Ag30 Ag16 105.648(14) . 2_556 ?
Ag33 Ag30 Ag16 96.344(13) 2_556 2_556 ?
S24 Ag30 Ag16 49.27(2) 2_556 2_556 ?
S24 Ag30 Ag16 150.36(3) . 2_556 ?
Ag32 Ag30 Ag16 75.023(12) . 2_556 ?
Ag16 Ag30 Ag16 150.05(2) . 2_556 ?
S20 Ag31 S31 162.69(4) 4_556 . ?
S20 Ag31 Ag29 80.88(3) 4_556 4_556 ?
S31 Ag31 Ag29 83.97(2) . 4_556 ?
S20 Ag31 S16 84.58(4) 4_556 4_546 ?
S31 Ag31 S16 97.36(3) . 4_546 ?
Ag29 Ag31 S16 124.78(3) 4_556 4_546 ?
S20 Ag31 S27 102.51(3) 4_556 . ?
S31 Ag31 S27 92.78(3) . . ?
Ag29 Ag31 S27 123.28(2) 4_556 . ?
S16 Ag31 S27 111.83(4) 4_546 . ?
S20 Ag31 Ag22 130.79(3) 4_556 . ?
S31 Ag31 Ag22 65.83(2) . . ?
Ag29 Ag31 Ag22 146.855(18) 4_556 . ?
S16 Ag31 Ag22 74.76(3) 4_546 . ?
S27 Ag31 Ag22 49.57(2) . . ?
S20 Ag31 Ag25 58.84(3) 4_556 4_546 ?
S31 Ag31 Ag25 133.95(3) . 4_546 ?
Ag29 Ag31 Ag25 138.789(17) 4_556 4_546 ?
S16 Ag31 Ag25 48.89(2) 4_546 4_546 ?
S27 Ag31 Ag25 77.47(3) . 4_546 ?
Ag22 Ag31 Ag25 74.31(2) . 4_546 ?
S20 Ag31 Ag18 108.42(3) 4_556 . ?
S31 Ag31 Ag18 61.30(3) . . ?
Ag29 Ag31 Ag18 83.524(14) 4_556 . ?
S16 Ag31 Ag18 51.72(2) 4_546 . ?
S27 Ag31 Ag18 142.08(2) . . ?
Ag22 Ag31 Ag18 92.971(14) . . ?
Ag25 Ag31 Ag18 100.207(16) 4_546 . ?
S20 Ag31 Ag26 67.95(3) 4_556 4_556 ?
S31 Ag31 Ag26 117.70(3) . 4_556 ?
Ag29 Ag31 Ag26 80.625(13) 4_556 4_556 ?
S16 Ag31 Ag26 139.74(3) 4_546 4_556 ?
S27 Ag31 Ag26 51.353(19) . 4_556 ?
Ag22 Ag31 Ag26 100.912(15) . 4_556 ?
Ag25 Ag31 Ag26 91.042(14) 4_546 4_556 ?
Ag18 Ag31 Ag26 164.11(2) . 4_556 ?
S29 Ag32 S29 174.75(6) . 2_556 ?
S29 Ag32 Ag30 92.63(3) . . ?
S29 Ag32 Ag30 92.63(3) 2_556 . ?
S29 Ag32 Hg1 67.93(3) . 2_556 ?
S29 Ag32 Hg1 112.27(3) 2_556 2_556 ?
Ag30 Ag32 Hg1 87.964(13) . 2_556 ?
S29 Ag32 Ag27 99.97(3) . . ?
S29 Ag32 Ag27 75.54(3) 2_556 . ?
Ag30 Ag32 Ag27 146.605(10) . . ?
Hg1 Ag32 Ag27 125.43(2) 2_556 . ?
S29 Ag32 Ag27 75.54(3) . 2_556 ?
S29 Ag32 Ag27 99.97(3) 2_556 2_556 ?
Ag30 Ag32 Ag27 146.605(10) . 2_556 ?
Hg1 Ag32 Ag27 58.642(12) 2_556 2_556 ?
Ag27 Ag32 Ag27 66.79(2) . 2_556 ?
S22 Ag33 S31 101.34(4) . . ?
S22 Ag33 S24 161.46(5) . 2_556 ?
S31 Ag33 S24 95.82(4) . 2_556 ?
S22 Ag33 Ag30 104.60(3) . . ?
S31 Ag33 Ag30 147.42(3) . . ?
S24 Ag33 Ag30 62.23(3) 2_556 . ?
S22 Ag33 Ag34 76.61(3) . . ?
S31 Ag33 Ag34 109.22(3) . . ?
S24 Ag33 Ag34 91.21(3) 2_556 . ?
Ag30 Ag33 Ag34 95.791(17) . . ?
S25 Ag34 S25 160.87(6) . 2_556 ?
S25 Ag34 Ag33 112.39(3) . . ?
S25 Ag34 Ag33 82.40(3) 2_556 . ?
S25 Ag34 Ag33 82.40(3) . 2_556 ?
S25 Ag34 Ag33 112.39(3) 2_556 2_556 ?
Ag33 Ag34 Ag33 83.14(2) . 2_556 ?
S25 Ag34 Ag20 80.43(3) . . ?
S25 Ag34 Ag20 80.43(3) 2_556 . ?
Ag33 Ag34 Ag20 138.429(12) . . ?
Ag33 Ag34 Ag20 138.429(12) 2_556 . ?
S10 As1 S5 98.06(5) . . ?
S10 As1 S2 98.44(7) . . ?
S5 As1 S2 99.12(5) . . ?
S9 As2 S8 102.30(6) . . ?
S9 As2 S1 98.77(5) . . ?
S8 As2 S1 95.06(5) . . ?
S4 As3 S7 98.61(6) . . ?
S4 As3 S3 100.04(5) . . ?
S7 As3 S3 98.26(5) . . ?
S6 As4 S11 101.34(5) . . ?
S6 As4 S13 96.26(6) . . ?
S11 As4 S13 100.71(5) . . ?
S16 As5 S21 101.16(4) . . ?
S16 As5 S26 95.45(5) . 4_556 ?
S21 As5 S26 100.07(5) . 4_556 ?
S22 As6 S24 101.21(5) . . ?
S22 As6 S25 98.87(5) . . ?
S24 As6 S25 99.83(4) . . ?
S17 As7 S23 102.17(6) 2_556 . ?
S17 As7 S29 95.78(5) 2_556 2_556 ?
S23 As7 S29 98.90(4) . 2_556 ?
S28 As8 S27 99.51(4) 4_546 . ?
S28 As8 S30 98.60(5) 4_546 4_546 ?
S27 As8 S30 100.57(5) . 4_546 ?
As2 S1 Ag15 114.51(7) . . ?
As2 S1 Ag5 105.29(5) . 1_565 ?
Ag15 S1 Ag5 120.63(5) . 1_565 ?
As2 S1 Ag3 100.41(4) . 2 ?
Ag15 S1 Ag3 108.35(5) . 2 ?
Ag5 S1 Ag3 105.45(6) 1_565 2 ?
As1 S2 Ag19 118.44(6) . . ?
As1 S2 Ag9 103.63(5) . . ?
Ag19 S2 Ag9 110.28(7) . . ?
As1 S2 Ag6 102.92(7) . . ?
Ag19 S2 Ag6 119.78(6) . . ?
Ag9 S2 Ag6 99.03(5) . . ?
As3 S3 Ag9 104.41(5) . 4_556 ?
As3 S3 Ag18 113.68(7) . . ?
Ag9 S3 Ag18 103.29(4) 4_556 . ?
As3 S3 Ag10 107.49(4) . . ?
Ag9 S3 Ag10 110.74(6) 4_556 . ?
Ag18 S3 Ag10 116.53(4) . . ?
As3 S4 Ag3 104.66(4) . 1_556 ?
As3 S4 Ag23 110.08(4) . . ?
Ag3 S4 Ag23 110.81(6) 1_556 . ?
As3 S4 Ag11 108.93(6) . . ?
Ag3 S4 Ag11 103.01(4) 1_556 . ?
Ag23 S4 Ag11 118.33(4) . . ?
As1 S5 Ag16 114.95(7) . . ?
As1 S5 Ag4 108.29(4) . . ?
Ag16 S5 Ag4 113.78(4) . . ?
As1 S5 Ag7 107.61(4) . 2_556 ?
Ag16 S5 Ag7 102.84(4) . 2_556 ?
Ag4 S5 Ag7 108.96(6) . 2_556 ?
As4 S6 Ag5 116.49(5) . 2_556 ?
As4 S6 Ag13 113.62(5) . . ?
Ag5 S6 Ag13 105.91(6) 2_556 . ?
As4 S6 Ag11 102.64(7) . 1_545 ?
Ag5 S6 Ag11 118.21(5) 2_556 1_545 ?
Ag13 S6 Ag11 98.88(4) . 1_545 ?
As3 S7 Ag17 114.07(5) . . ?
As3 S7 Ag8 100.49(6) . . ?
Ag17 S7 Ag8 103.36(4) . . ?
As3 S7 Ag4 109.75(5) . 2_556 ?
Ag17 S7 Ag4 114.89(7) . 2_556 ?
Ag8 S7 Ag4 113.27(4) . 2_556 ?
As2 S8 Ag6 107.58(6) . 1_565 ?
As2 S8 Ag28 109.11(4) . . ?
Ag6 S8 Ag28 105.76(4) 1_565 . ?
As2 S8 Ag10 107.03(4) . 4_556 ?
Ag6 S8 Ag10 118.97(4) 1_565 4_556 ?
Ag28 S8 Ag10 108.14(5) . 4_556 ?
As2 S9 Ag14 117.08(6) . . ?
As2 S9 Ag12 100.60(5) . . ?
Ag14 S9 Ag12 107.89(6) . . ?
As2 S9 Ag2 109.79(6) . . ?
Ag14 S9 Ag2 117.22(5) . . ?
Ag12 S9 Ag2 101.65(5) . . ?
As1 S10 Ag2 104.02(7) . . ?
As1 S10 Ag1 110.29(5) . 4_546 ?
Ag2 S10 Ag1 113.94(5) . 4_546 ?
As1 S10 Ag24 109.01(5) . . ?
Ag2 S10 Ag24 105.52(5) . . ?
Ag1 S10 Ag24 113.49(7) 4_546 . ?
As4 S11 Ag26 116.48(7) . . ?
As4 S11 Ag1 103.83(4) . 1_545 ?
Ag26 S11 Ag1 116.74(4) . 1_545 ?
As4 S11 Ag12 104.64(4) . 4_546 ?
Ag26 S11 Ag12 106.55(4) . 4_546 ?
Ag1 S11 Ag12 107.74(6) 1_545 4_546 ?
Ag9 S12 Ag11 102.46(4) 4 1_554 ?
Ag9 S12 Ag12 105.73(6) 4 . ?
Ag11 S12 Ag12 91.02(4) 1_554 . ?
Ag9 S12 Ag1 96.01(3) 4 1_554 ?
Ag11 S12 Ag1 73.75(4) 1_554 1_554 ?
Ag12 S12 Ag1 155.81(6) . 1_554 ?
Ag9 S12 Ag10 173.10(6) 4 4_556 ?
Ag11 S12 Ag10 77.95(4) 1_554 4_556 ?
Ag12 S12 Ag10 81.12(3) . 4_556 ?
Ag1 S12 Ag10 77.43(4) 1_554 4_556 ?
Ag9 S12 Ag8 99.71(5) 4 4_556 ?
Ag11 S12 Ag8 147.96(6) 1_554 4_556 ?
Ag12 S12 Ag8 104.93(4) . 4_556 ?
Ag1 S12 Ag8 81.20(4) 1_554 4_556 ?
Ag10 S12 Ag8 77.34(4) 4_556 4_556 ?
As4 S13 Ag7 108.16(4) . . ?
As4 S13 Ag21 112.34(4) . . ?
Ag7 S13 Ag21 114.95(6) . . ?
As4 S13 Ag8 106.62(6) . . ?
Ag7 S13 Ag8 95.95(4) . . ?
Ag21 S13 Ag8 117.33(4) . . ?
Ag4 S14 Ag4 78.64(4) 2 . ?
Ag4 S14 Ag3 90.761(14) 2 . ?
Ag4 S14 Ag3 166.14(4) . . ?
Ag4 S14 Ag3 166.14(4) 2 2 ?
Ag4 S14 Ag3 90.761(14) . 2 ?
Ag3 S14 Ag3 101.00(5) . 2 ?
Ag4 S14 Ag2 81.02(3) 2 . ?
Ag4 S14 Ag2 74.48(3) . . ?
Ag3 S14 Ag2 95.21(2) . . ?
Ag3 S14 Ag2 104.92(2) 2 . ?
Ag4 S14 Ag2 74.48(3) 2 2 ?
Ag4 S14 Ag2 81.02(3) . 2 ?
Ag3 S14 Ag2 104.92(2) . 2 ?
Ag3 S14 Ag2 95.21(2) 2 2 ?
Ag2 S14 Ag2 148.23(6) . 2 ?
Ag7 S15 Ag7 101.92(6) 1_554 2_556 ?
Ag7 S15 Ag6 103.02(2) 1_554 2 ?
Ag7 S15 Ag6 94.19(2) 2_556 2 ?
Ag7 S15 Ag6 94.19(2) 1_554 . ?
Ag7 S15 Ag6 103.02(2) 2_556 . ?
Ag6 S15 Ag6 152.60(8) 2 . ?
Ag7 S15 Ag5 89.588(14) 1_554 2 ?
Ag7 S15 Ag5 167.43(5) 2_556 2 ?
Ag6 S15 Ag5 78.13(4) 2 2 ?
Ag6 S15 Ag5 80.87(4) . 2 ?
Ag7 S15 Ag5 167.43(5) 1_554 . ?
Ag7 S15 Ag5 89.588(14) 2_556 . ?
Ag6 S15 Ag5 80.87(4) 2 . ?
Ag6 S15 Ag5 78.13(4) . . ?
Ag5 S15 Ag5 79.45(5) 2 . ?
As5 S16 Ag25 112.88(5) . . ?
As5 S16 Ag18 102.19(4) . 4_556 ?
Ag25 S16 Ag18 135.56(5) . 4_556 ?
As5 S16 Ag28 98.01(5) . . ?
Ag25 S16 Ag28 87.26(4) . . ?
Ag18 S16 Ag28 114.65(5) 4_556 . ?
As5 S16 Ag31 131.80(7) . 4_556 ?
Ag25 S16 Ag31 68.22(3) . 4_556 ?
Ag18 S16 Ag31 68.18(3) 4_556 4_556 ?
Ag28 S16 Ag31 129.51(5) . 4_556 ?
As7 S17 Ag27 113.46(5) 2_556 . ?
As7 S17 Ag28 103.23(5) 2_556 1_545 ?
Ag27 S17 Ag28 93.19(4) . 1_545 ?
As7 S17 Ag19 104.93(5) 2_556 . ?
Ag27 S17 Ag19 124.73(5) . . ?
Ag28 S17 Ag19 115.38(4) 1_545 . ?
Fe2 S18 Ag20 121.99(4) . . ?
Fe2 S18 Ag25 78.23(4) . . ?
Ag20 S18 Ag25 142.21(4) . . ?
Fe2 S18 Ag27 145.98(6) . 1_565 ?
Ag20 S18 Ag27 71.88(3) . 1_565 ?
Ag25 S18 Ag27 75.35(3) . 1_565 ?
Fe1 S19 Ag30 123.20(4) . . ?
Fe1 S19 Ag19 71.86(3) . . ?
Ag30 S19 Ag19 137.84(6) . . ?
Fe1 S19 Ag24 126.02(5) . . ?
Ag30 S19 Ag24 110.31(5) . . ?
Ag19 S19 Ag24 63.75(2) . . ?
Fe1 S19 Ag22 76.66(4) . . ?
Ag30 S19 Ag22 125.57(4) . . ?
Ag19 S19 Ag22 95.20(4) . . ?
Ag24 S19 Ag22 78.34(3) . . ?
Fe1 S19 Ag16 123.80(5) . . ?
Ag30 S19 Ag16 74.72(4) . . ?
Ag19 S19 Ag16 65.85(3) . . ?
Ag24 S19 Ag16 62.19(3) . . ?
Ag22 S19 Ag16 140.42(4) . . ?
Ag31 S20 Fe1 122.45(4) 4_546 . ?
Ag31 S20 Ag25 74.16(3) 4_546 1_545 ?
Fe1 S20 Ag25 147.80(5) . 1_545 ?
Ag31 S20 Ag27 145.40(4) 4_546 . ?
Fe1 S20 Ag27 77.92(4) . . ?
Ag25 S20 Ag27 75.77(3) 1_545 . ?
As5 S21 Ag26 105.06(5) . 4_556 ?
As5 S21 Ag29 98.01(5) . 4_556 ?
Ag26 S21 Ag29 98.70(5) 4_556 4_556 ?
As5 S21 Ag14 102.33(5) . . ?
Ag26 S21 Ag14 119.28(5) 4_556 . ?
Ag29 S21 Ag14 129.45(4) 4_556 . ?
As6 S22 Ag33 115.56(4) . . ?
As6 S22 Ag24 101.96(4) . . ?
Ag33 S22 Ag24 92.08(4) . . ?
As6 S22 Ag14 103.46(4) . . ?
Ag33 S22 Ag14 124.19(5) . . ?
Ag24 S22 Ag14 117.85(4) . . ?
As7 S23 Ag13 104.74(6) . . ?
As7 S23 Ag27 108.96(5) . . ?
Ag13 S23 Ag27 94.50(5) . . ?
As7 S23 Ag15 100.64(5) . 2_546 ?
Ag13 S23 Ag15 118.50(6) . 2_546 ?
Ag27 S23 Ag15 127.80(6) . 2_546 ?
As6 S24 Ag17 103.38(6) . 2_556 ?
As6 S24 Ag16 102.00(4) . . ?
Ag17 S24 Ag16 116.88(5) 2_556 . ?
As6 S24 Ag33 107.99(5) . 2_556 ?
Ag17 S24 Ag33 87.47(4) 2_556 2_556 ?
Ag16 S24 Ag33 135.45(5) . 2_556 ?
As6 S24 Ag30 122.38(7) . . ?
Ag17 S24 Ag30 129.71(4) 2_556 . ?
Ag16 S24 Ag30 75.33(4) . . ?
Ag33 S24 Ag30 60.94(3) 2_556 . ?
As6 S25 Ag34 97.69(5) . . ?
As6 S25 Ag15 104.61(4) . . ?
Ag34 S25 Ag15 99.87(5) . . ?
As6 S25 Ag23 102.97(5) . 2_556 ?
Ag34 S25 Ag23 127.43(4) . 2_556 ?
Ag15 S25 Ag23 120.12(5) . 2_556 ?
As5 S26 Ag22 111.73(5) 4_546 . ?
As5 S26 Ag17 103.21(5) 4_546 . ?
Ag22 S26 Ag17 97.24(4) . . ?
As5 S26 Ag21 99.06(4) 4_546 . ?
Ag22 S26 Ag21 125.92(5) . . ?
Ag17 S26 Ag21 118.13(4) . . ?
As8 S27 Ag22 109.04(4) . . ?
As8 S27 Ag26 101.00(4) . 4_556 ?
Ag22 S27 Ag26 134.31(5) . 4_556 ?
As8 S27 Ag24 99.36(4) . . ?
Ag22 S27 Ag24 89.32(4) . . ?
Ag26 S27 Ag24 119.20(4) 4_556 . ?
As8 S27 Ag31 129.97(6) . . ?
Ag22 S27 Ag31 66.16(3) . . ?
Ag26 S27 Ag31 68.17(3) 4_556 . ?
Ag24 S27 Ag31 129.21(4) . . ?
As8 S28 Ag29 101.73(6) 4_556 4_556 ?
As8 S28 Ag19 104.82(6) 4_556 4_556 ?
Ag29 S28 Ag19 124.06(4) 4_556 4_556 ?
As8 S28 Ag18 105.95(5) 4_556 . ?
Ag29 S28 Ag18 100.29(5) 4_556 . ?
Ag19 S28 Ag18 117.81(5) 4_556 . ?
As7 S29 Ag32 112.13(5) 2_556 . ?
As7 S29 Ag16 102.58(4) 2_556 . ?
Ag32 S29 Ag16 98.20(5) . . ?
As7 S29 Ag21 98.56(4) 2_556 2_556 ?
Ag32 S29 Ag21 128.48(4) . 2_556 ?
Ag16 S29 Ag21 114.73(4) . 2_556 ?
As8 S30 Ag25 108.52(5) 4_556 . ?
As8 S30 Ag13 98.98(5) 4_556 1_565 ?
Ag25 S30 Ag13 93.16(4) . 1_565 ?
As8 S30 Ag23 98.98(5) 4_556 . ?
Ag25 S30 Ag23 133.12(5) . . ?
Ag13 S30 Ag23 119.59(4) 1_565 . ?
Fe2 S31 Ag31 107.35(3) . . ?
Fe2 S31 Ag33 81.56(4) . . ?
Ag31 S31 Ag33 129.65(3) . . ?
Fe2 S31 Ag23 76.51(3) . . ?
Ag31 S31 Ag23 125.76(4) . . ?
Ag33 S31 Ag23 104.58(3) . . ?
Fe2 S31 Ag18 120.04(4) . . ?
Ag31 S31 Ag18 69.89(3) . . ?
Ag33 S31 Ag18 147.89(3) . . ?
Ag23 S31 Ag18 63.00(2) . . ?
Fe2 S31 Ag17 133.02(4) . . ?
Ag31 S31 Ag17 117.13(4) . . ?
Ag33 S31 Ag17 81.58(3) . . ?
Ag23 S31 Ag17 65.99(2) . . ?
Ag18 S31 Ag17 66.31(2) . . ?
 
_diffrn_measured_fraction_theta_max    0.997
_diffrn_reflns_theta_full              34.84
_diffrn_measured_fraction_theta_full   0.995
_refine_diff_density_max    1.130
_refine_diff_density_min   -1.396
_refine_diff_density_rms    0.168
